Pulse electrodeposition of Prussian Blue thin films
Identifieur interne : 000639 ( Main/Repository ); précédent : 000638; suivant : 000640Pulse electrodeposition of Prussian Blue thin films
Auteurs : RBID : Pascal:13-0284991Descripteurs français
- Pascal (Inist)
- Dépôt électrolytique, Couche mince, Densité courant, Propriété électrochimique, Spectroscopie impédance électrochimique, Voltammétrie cyclique, Revêtement électrodéposé, Transfert charge, Coefficient diffusion, Plan expérience, Morphologie, Substrat oxyde d'indium et de zinc, Substrat verre, 8115P, 8245M, 8245F.
English descriptors
- KwdEn :
Abstract
The effects of pulse electrodeposition parameters like peak current density and frequency on the electrochemical properties of Prussian Blue thin films were investigated. Electrochemical Impedance Spectroscopy, Cyclic Voltammetry and Chronoamperometry tests were carried out on Prussian Blue thin films which were pulse electrodeposited on Indium Tin Oxide coated glass substrates. The results showed that increase in the peak current densities and using higher pulsating frequencies during electrodeposition decreases the charge transfer resistance of the thin films while the diffusion coefficient of electroactive species in the films is increased as a consequence of using the same pulsating parameters. In addition, pulse electrodeposition technique does not alter deposition mechanism and morphology of the Prussian Blue thin films.
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Bahrololoom</name><affiliation wicri:level="1"><inist:fA14 i1="01"><s1>Department of Materials Science and Engineering, School of Engineering, Shiraz University</s1><s2>71348-15939 Shiraz</s2><s3>IRN</s3><sZ>1 aut.</sZ><sZ>2 aut.</sZ></inist:fA14><country>Iran</country><wicri:noRegion>71348-15939 Shiraz</wicri:noRegion></affiliation></author></titleStmt><publicationStmt><idno type="inist">13-0284991</idno><date when="2013">2013</date><idno type="stanalyst">PASCAL 13-0284991 INIST</idno><idno type="RBID">Pascal:13-0284991</idno><idno type="wicri:Area/Main/Corpus">000870</idno><idno type="wicri:Area/Main/Repository">000639</idno></publicationStmt><seriesStmt><idno type="ISSN">0040-6090</idno><title level="j" type="abbreviated">Thin solid films</title><title level="j" type="main">Thin solid films</title></seriesStmt></fileDesc><profileDesc><textClass><keywords scheme="KwdEn" xml:lang="en"><term>Charge transfer</term><term>Current density</term><term>Cyclic voltammetry</term><term>Diffusion coefficient</term><term>Electrochemical impedance spectroscopy</term><term>Electrochemical properties</term><term>Electrodeposited coatings</term><term>Electrodeposition</term><term>Experimental design</term><term>Morphology</term><term>Thin films</term></keywords><keywords scheme="Pascal" xml:lang="fr"><term>Dépôt électrolytique</term><term>Couche mince</term><term>Densité courant</term><term>Propriété électrochimique</term><term>Spectroscopie impédance électrochimique</term><term>Voltammétrie cyclique</term><term>Revêtement électrodéposé</term><term>Transfert charge</term><term>Coefficient diffusion</term><term>Plan expérience</term><term>Morphologie</term><term>Substrat oxyde d'indium et de zinc</term><term>Substrat verre</term><term>8115P</term><term>8245M</term><term>8245F</term></keywords></textClass></profileDesc></teiHeader><front><div type="abstract" xml:lang="en">The effects of pulse electrodeposition parameters like peak current density and frequency on the electrochemical properties of Prussian Blue thin films were investigated. Electrochemical Impedance Spectroscopy, Cyclic Voltammetry and Chronoamperometry tests were carried out on Prussian Blue thin films which were pulse electrodeposited on Indium Tin Oxide coated glass substrates. The results showed that increase in the peak current densities and using higher pulsating frequencies during electrodeposition decreases the charge transfer resistance of the thin films while the diffusion coefficient of electroactive species in the films is increased as a consequence of using the same pulsating parameters. 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